TA Instruments

AR1756-0013f

15/03/2013 15:15:34

Sample name	ASW Blank coupon#20 + DI + beads 50rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	13 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:15:34

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 100.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	99.98	-700.14	10000	20.0	0.4934	0.992	-228.2	125.0	-1.826	2010	87.5556	0.1287	109.44	10944	3.411E-3	0.0	0.0
1.9920	99.99	113.13	10000	20.0	0.4896	1.992	36.88	125.0	0.2950	1995	175.5470	0.1277	219.43	21943	3.411E-3	0.0	0.0
3.0120	100.0	113.11	10000	20.0	0.4877	3.012	36.87	125.0	0.2949	1987	263.4970	0.1272	329.37	32937	3.411E-3	0.1	0.1
3.9920	100.0	114.09	10000	20.0	0.4875	3.992	37.19	125.0	0.2975	1986	395.4620	0.1271	494.33	49433	3.411E-3	0.1	0.1
4.9920	100.0	113.19	10000	20.0	0.4894	4.992	36.89	125.0	0.2951	1994	483.4040	0.1276	604.26	60426	3.411E-3	0.1	0.1
6.0120	100.0	112.55	10000	20.0	0.4896	6.012	36.68	125.0	0.2935	1995	571.3390	0.1277	714.17	71417	3.411E-3	0.1	0.1
7.0120	100.0	113.31	10000	20.0	0.4857	7.012	36.93	125.0	0.2955	1979	659.3390	0.1267	824.17	82417	3.411E-3	0.1	0.1
7.9880	100.0	113.89	10000	20.0	0.4867	7.988	37.12	125.0	0.2970	1983	791.2940	0.1269	989.12	98912	3.411E-3	0.1	0.1
8.9920	100.0	113.24	10000	20.0	0.4847	8.992	36.91	125.0	0.2953	1975	879.8120	0.1264	1099.8	1.0998E5	3.411E-3	0.1	0.1
9.9960	100.0	112.11	10000	20.0	0.4847	9.996	36.54	125.0	0.2923	1975	967.1410	0.1264	1208.9	1.2089E5	3.411E-3	0.2	0.2
10.992	100.0	111.87	10000	20.0	0.4819	10.992	36.46	125.0	0.2917	1963	1100.0000	0.1256	1375.0	1.3750E5	3.411E-3	0.2	0.2
11.992	100.0	112.03	10000	20.0	0.4831	11.992	36.52	125.0	0.2921	1968	1187.1000	0.1260	1483.9	1.4839E5	3.411E-3	0.2	0.2
12.992	100.0	111.55	10000	20.0	0.4853	12.992	36.36	125.0	0.2909	1977	1275.0500	0.1266	1593.8	1.5938E5	3.411E-3	0.2	0.2
13.992	100.0	110.53	10000	20.0	0.4829	13.992	36.03	125.0	0.2882	1967	1363.3700	0.1259	1704.2	1.7042E5	3.411E-3	0.2	0.2
14.992	100.0	111.45	10000	20.0	0.4837	14.992	36.33	125.0	0.2906	1971	1494.9399	0.1261	1868.7	1.8687E5	3.411E-3	0.2	0.2
15.992	100.0	110.23	10000	20.0	0.4827	15.992	35.93	125.0	0.2874	1967	1582.8900	0.1259	1978.6	1.9786E5	3.411E-3	0.3	0.3
16.992	100.0	111.78	10000	20.0	0.4837	16.992	36.43	125.0	0.2915	1971	1672.0800	0.1261	2090.1	2.0901E5	3.411E-3	0.3	0.3
17.992	100.0	112.45	10000	20.0	0.4859	17.992	36.65	125.0	0.2932	1980	1760.5000	0.1267	2200.6	2.2006E5	3.411E-3	0.3	0.3
18.992	100.0	112.35	10000	20.0	0.4849	18.992	36.62	125.0	0.2930	1976	1890.7600	0.1264	2363.5	2.3635E5	3.411E-3	0.3	0.3
19.992	100.0	110.58	10000	20.0	0.4825	19.992	36.04	125.0	0.2884	1966	1978.7700	0.1258	2473.5	2.4735E5	3.411E-3	0.3	0.3
20.992	100.0	110.62	10000	20.0	0.4823	20.992	36.06	125.0	0.2885	1965	2066.6899	0.1258	2583.4	2.5834E5	3.411E-3	0.3	0.3
21.996	100.0	111.14	10000	20.0	0.4825	21.996	36.23	125.0	0.2898	1966	2199.4099	0.1258	2749.3	2.7493E5	3.411E-3	0.4	0.4
22.992	100.0	111.31	10000	20.0	0.4819	22.992	36.28	125.0	0.2902	1963	2286.6101	0.1257	2858.3	2.8583E5	3.411E-3	0.4	0.4
23.992	100.0	110.73	10000	20.0	0.4839	23.992	36.09	125.0	0.2887	1972	2374.5701	0.1262	2968.2	2.9682E5	3.411E-3	0.4	0.4
24.992	100.0	109.77	10000	20.0	0.4766	24.992	35.78	125.0	0.2862	1942	2462.5500	0.1243	3078.2	3.0782E5	3.411E-3	0.4	0.4
25.992	100.0	110.71	10000	20.0	0.4815	25.992	36.09	125.0	0.2887	1962	2594.5100	0.1255	3243.1	3.2431E5	3.411E-3	0.4	0.4
26.996	100.0	111.31	10000	20.0	0.4811	26.996	36.28	125.0	0.2902	1960	2682.4399	0.1254	3353.1	3.3531E5	3.411E-3	0.4	0.4
27.992	100.0	111.14	10000	20.0	0.4802	27.992	36.23	125.0	0.2898	1957	2770.4399	0.1252	3463.1	3.4631E5	3.411E-3	0.5	0.5
28.992	100.0	109.99	10000	20.0	0.4778	28.992	35.85	125.0	0.2868	1947	2858.7700	0.1246	3573.5	3.5735E5	3.411E-3	0.5	0.5
29.992	100.0	110.15	10000	20.0	0.4762	29.992	35.90	125.0	0.2872	1940	2990.3401	0.1242	3737.9	3.7379E5	3.411E-3	0.5	0.5
30.992	100.0	110.34	10000	20.0	0.4764	30.992	35.96	125.0	0.2877	1941	3078.2200	0.1242	3847.8	3.8478E5	3.411E-3	0.5	0.5
31.992	100.0	109.92	10000	20.0	0.4774	31.992	35.83	125.0	0.2866	1945	3166.2700	0.1245	3957.8	3.9578E5	3.411E-3	0.5	0.5
32.992	100.0	108.98	10000	20.0	0.4764	32.992	35.52	125.0	0.2842	1941	3304.4800	0.1242	4130.6	4.1306E5	3.411E-3	0.5	0.5
33.992	100.0	111.51	10000	20.0	0.4772	33.992	36.35	125.0	0.2908	1944	3386.1101	0.1244	4232.6	4.2326E5	3.411E-3	0.6	0.6
34.992	100.0	111.25	10000	20.0	0.4772	34.992	36.26	125.0	0.2901	1944	3474.1001	0.1244	4342.6	4.3426E5	3.411E-3	0.6	0.6
35.992	100.0	110.68	10000	20.0	0.4782	35.992	36.08	125.0	0.2886	1948	3562.7500	0.1247	4453.4	4.4534E5	3.411E-3	0.6	0.6
36.996	100.0	110.00	10000	20.0	0.4784	36.996	35.85	125.0	0.2868	1949	3693.9800	0.1248	4617.5	4.6175E5	3.411E-3	0.6	0.6
37.992	100.0	108.02	10000	20.0	0.4770	37.992	35.21	125.0	0.2817	1943	3781.9199	0.1244	4727.4	4.7274E5	3.411E-3	0.6	0.6
38.992	100.0	108.91	10000	20.0	0.4762	38.992	35.50	125.0	0.2840	1940	3870.2000	0.1242	4837.8	4.8378E5	3.411E-3	0.6	0.6
39.992	100.0	108.47	10000	20.0	0.4758	39.992	35.36	125.0	0.2828	1938	3957.8701	0.1241	4947.3	4.9473E5	3.411E-3	0.7	0.7
40.992	100.0	109.01	10000	20.0	0.4806	40.992	35.53	125.0	0.2843	1958	4089.7800	0.1253	5112.2	5.1122E5	3.411E-3	0.7	0.7
42.000	100.0	107.82	10000	20.0	0.4778	42.000	35.14	125.0	0.2812	1947	4177.7798	0.1246	5222.2	5.2222E5	3.411E-3	0.7	0.7
42.992	100.0	110.27	10000	20.0	0.4742	42.992	35.94	125.0	0.2875	1932	4265.7700	0.1236	5332.2	5.3322E5	3.411E-3	0.7	0.7
43.992	100.0	109.07	10000	20.0	0.4748	43.992	35.55	125.0	0.2844	1934	4398.0898	0.1238	5497.6	5.4976E5	3.411E-3	0.7	0.7
44.992	100.0	110.16	10000	20.0	0.4762	44.992	35.91	125.0	0.2873	1940	4485.6602	0.1242	5607.1	5.6071E5	3.411E-3	0.7	0.7
45.992	100.0	109.10	10000	20.0	0.4721	45.992	35.56	125.0	0.2845	1924	4573.6201	0.1231	5717.0	5.7170E5	3.411E-3	0.8	0.8
46.992	100.0	109.28	10000	20.0	0.4748	46.992	35.62	125.0	0.2850	1934	4661.6001	0.1238	5827.0	5.8270E5	3.411E-3	0.8	0.8
47.992	100.0	109.58	10000	20.0	0.4740	47.992	35.72	125.0	0.2858	1931	4793.6602	0.1236	5992.1	5.9921E5	3.411E-3	0.8	0.8
48.992	100.0	110.21	10000	20.0	0.4733	48.992	35.92	125.0	0.2874	1929	4881.5098	0.1234	6101.9	6.1019E5	3.411E-3	0.8	0.8
49.992	100.0	108.71	10000	20.0	0.4711	49.992	35.43	125.0	0.2835	1919	4969.6299	0.1228	6212.0	6.2120E5	3.411E-3	0.8	0.8
50.992	100.0	109.90	10000	20.0	0.4727	50.992	35.82	125.0	0.2866	1926	5057.4302	0.1233	6321.8	6.3218E5	3.411E-3	0.8	0.8
51.992	100.0	109.31	10000	20.0	0.4695	51.992	35.63	125.0	0.2850	1913	5189.3398	0.1224	6486.7	6.4867E5	3.411E-3	0.9	0.9
52.992	100.0	109.96	10000	20.0	0.4713	52.992	35.84	125.0	0.2867	1920	5277.2798	0.1229	6596.6	6.5966E5	3.411E-3	0.9	0.9
53.992	100.0	109.87	10000	20.0	0.4735	53.992	35.81	125.0	0.2865	1929	5365.7402	0.1235	6707.2	6.7072E5	3.411E-3	0.9	0.9
54.992	100.0	110.16	10000	20.0	0.4699	54.992	35.91	125.0	0.2873	1915	5497.1899	0.1225	6871.5	6.8715E5	3.411E-3	0.9	0.9
55.992	100.0	110.78	10000	20.0	0.4733	55.992	36.11	125.0	0.2889	1929	5585.1401	0.1234	6981.4	6.9814E5	3.411E-3	0.9	0.9
56.992	100.0	109.23	10000	20.0	0.4705	56.992	35.60	125.0	0.2848	1917	5673.9702	0.1227	7092.5	7.0925E5	3.411E-3	0.9	0.9
57.992	100.0	111.05	10000	20.0	0.4746	57.992	36.20	125.0	0.2896	1934	5761.0898	0.1237	7201.4	7.2014E5	3.411E-3	1.0	1.0
58.992	100.0	109.34	10000	20.0	0.4727	58.992	35.64	125.0	0.2851	1926	5893.0698	0.1233	7366.3	7.3663E5	3.411E-3	1.0	1.0
59.992	100.0	112.09	10000	20.0	0.4727	59.992	36.54	125.0	0.2923	1926	5981.6802	0.1233	7477.1	7.4771E5	3.411E-3	1.0	1.0

